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filingDate 1981-05-14-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 1985-08-30-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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publicationDate 1985-08-30-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber SU-1176835-A3
titleOfInvention Method of producing methane sulphochloride
abstract 1. METHOD OF OBTAINING META OF SULFOHLORIDE by reacting dime thyl disulfide with chlorine in the presence of a concentrated solution of hydrochloric acid in a homogeneous medium at natural temperature, separating the target product by decantation and recycling the hydrochloric acid solution, characterized in that, in order to improve the performance of the process, the interaction lead by emulsifying dimethyl disulfide in a concentrated hydrochloric acid solution to form an emulsion with droplets with a diameter of 1–20 µm through which chlorine is passed. The reaction mixture was continuously recirculated from 2/3 to 5/6 of its volume between the reaction zone and the decantation zone, the mixture was not allowed to pass through the cooling system at such a rate, and phase separation did not occur. 36 /,
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Total number of triples: 30.