http://rdf.ncbi.nlm.nih.gov/pubchem/patent/SE-8207515-D0

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http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/A61K36-00
filingDate 1982-12-30-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_aa73b5614b032f8c190c0a7b77852292
publicationDate 1982-12-30-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber SE-8207515-D0
titleOfInvention PROCEDURE FOR THE EXTRACTION OF LAXATIVE SOCIETIES OF SENNED DRUGS
abstract The present invention provides a process for obtaining laxative compounds from senna drug, wherein a) the senna drug is extracted with aqueous methanol by countercurrent percolation and the extract concentrated at a temperature of >/=50 DEG C. until the methanol has been completely removed from the extract; b) the extract obtained is purified by continuous liquid-liquid extraction with an organic solvent; c) the refined material (raffinate) obtained is transferred to a crystallisation apparatus, acidified, while stirring, to a pH of 1.5 to 2.0, seeded with sennoside crystals, left to crystallise while stirring and the crystalline crude sennoside obtained separated off; d) whereafter, the crude senno- dies are, if desired, recrystallised and optionally e) 10 parts by weight of the mother liquor from c) mixed, while stirring, with 2 parts by weight of sodium chloride and the semi-solid mass coagulated on the surface is decanted off, washed and optionally extracted with 95% methanol and the methanol fraction concentrated and the residue dried. n
priorityDate 1982-01-05-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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Total number of triples: 27.