http://rdf.ncbi.nlm.nih.gov/pubchem/patent/RU-94046238-A

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classificationCPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C201-08
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classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C205-06
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C201-08
filingDate 1993-06-01-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_b0d84755036195afc733b2dc5f460ad8
publicationDate 1996-10-10-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber RU-94046238-A
titleOfInvention Method for production of dinitrotoluenes and product being prepared by this method
abstract This invention describes a toluene nitration method for producing dinitrotoluene, characterized by a liquid-phase nitration reaction, characterized in that it is a reaction of anhydrous nitric acid with toluene in a reactor at a reaction temperature of between 20 and 30 ° C. for a reaction time of less than 15 minutes with a molar ratio of nitric acid plus water to toluene between 10: 1 and 15: 1, the above reaction being carried out in the absence of sulfuric acid and any aprotic dipolar solvent during the reaction and in the absence of any aprotic dipole a solvent to stop the reaction to obtain the above dinitrotoluene in a mixture of products without nitrocresol impurity, followed by distillation in a vacuum of a mixture of products without using any aprotic dipolar solvent to remove unreacted nitric acid from the above mixture of products, thereby obtaining the above dinitrotoluene.
priorityDate 1992-06-17-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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Total number of triples: 29.