http://rdf.ncbi.nlm.nih.gov/pubchem/patent/RU-94046238-A
Outgoing Links
Predicate | Object |
---|---|
assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_5202091df9de019fc995f2d266f9ecc2 |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C201-08 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C205-06 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C205-06 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C201-08 |
filingDate | 1993-06-01-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_b0d84755036195afc733b2dc5f460ad8 |
publicationDate | 1996-10-10-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | RU-94046238-A |
titleOfInvention | Method for production of dinitrotoluenes and product being prepared by this method |
abstract | This invention describes a toluene nitration method for producing dinitrotoluene, characterized by a liquid-phase nitration reaction, characterized in that it is a reaction of anhydrous nitric acid with toluene in a reactor at a reaction temperature of between 20 and 30 ° C. for a reaction time of less than 15 minutes with a molar ratio of nitric acid plus water to toluene between 10: 1 and 15: 1, the above reaction being carried out in the absence of sulfuric acid and any aprotic dipolar solvent during the reaction and in the absence of any aprotic dipole a solvent to stop the reaction to obtain the above dinitrotoluene in a mixture of products without nitrocresol impurity, followed by distillation in a vacuum of a mixture of products without using any aprotic dipolar solvent to remove unreacted nitric acid from the above mixture of products, thereby obtaining the above dinitrotoluene. |
priorityDate | 1992-06-17-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 29.