http://rdf.ncbi.nlm.nih.gov/pubchem/patent/RU-2771232-C1
Outgoing Links
Predicate | Object |
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assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_52490458f9d42fb58ffd4beb4bbbc310 |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/A61P31-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/A61P35-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D207-32 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/A61P31-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/A61P35-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D207-32 |
filingDate | 2021-09-13-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2022-04-28-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_6756b19c1f259d195ad8561f69d456ac http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_6bcb74eb821aedffa92cb88f2091f74d http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_33fb07fa7e514303c05972ffc896fa29 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_e3af906c4963a4db03baa4d9ef611a7d http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_20e8b04989eb38b0837749b0f1b00745 |
publicationDate | 2022-04-28-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | RU-2771232-C1 |
titleOfInvention | Method for obtaining 2,5-bis(2-methoxyethyl)-3-alkyl(phenyl)-1h-pyrroles |
abstract | FIELD: chemistry. n SUBSTANCE: invention relates to a new method for the preparation of 3-alkyl(phenyl)-2,5-bis(2-methoxyethyl)-1H-pyrroles. A new method for the preparation of 3-alkyl(phenyl)-2,5-bis(2-methoxyethyl)-1H-pyrroles, which are of interest as initial synthons for the creation of biologically active compounds for medical and agricultural purposes, has been developed, which consists in the interaction of terminal acetylenes with 2 -fold excess of 3-methoxypropionitrile, 2.5-fold excess of ethylaluminum dichloride (EtAlCl2) in the presence of magnesium and Cp 2 TiCl 2 catalyst at 60°C in an argon atmosphere and atmospheric pressure for 8-12 h. Yield of 2,5-bis(2-methoxyethyl )-3-alkyl(phenyl)-1H-pyrroles (1) is 50-72%. n EFFECT: creation of a new method for the preparation of 3-alkyl(phenyl)-2,5-bis(2-methoxyethyl)-1H-pyrroles. n 1 cl, 1 ex, 1 tbl |
priorityDate | 2021-09-13-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 42.