http://rdf.ncbi.nlm.nih.gov/pubchem/patent/RU-2740667-C1

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assignee http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_99cd2888b2026702c522c60b1544ff90
classificationCPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/B01J29-06
http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C01B39-02
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/B01J29-06
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C01B39-02
filingDate 2019-12-13-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2021-01-19-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_a3c46425c1e2d9ae762c4eba4ae1521b
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_0d2f2fe6f02b23b54326ba3e94d9fd2d
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_23278631a01bd5232717621f6b9a8948
publicationDate 2021-01-19-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber RU-2740667-C1
titleOfInvention Method of producing high-module zeolite mcm-22 with high degree of crystallinity
abstract FIELD: chemistry.SUBSTANCE: invention relates to production of zeolites and can be used to produce catalysts based on molecular sieves, particularly for alkylation or transalkylation. Method of producing high-module zeolite MCM-22 involves mixing components - silicon source, aluminium source, sodium source and template in molar ratio SiO2/Al2O3- 40–70, crystallisation under conditions of mixing in autoclave at high temperature, recovering crystals of zeolite by filtration and washing with water and calcining the recovered zeolite at calcination temperature of 550–600 °C. Components are additionally added with sodium fluoride to molar ratio F/SiO2equal to 0.1–0.3. Crystallization is carried out for 9–11 days at temperature 150–170 °C. Desiccated zeolite is calcined in two steps - first at temperature of 300 °C for 1–3 hours, then at temperature of 550–600 °C for 1–6 hours.EFFECT: higher output of highly crystalline zeolite to 47–62 %.5 cl, 1 dwg, 1 tbl, 13 ex
priorityDate 2019-12-13-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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