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filingDate 2016-07-11-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2017-06-02-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_d870d4f8eed1d1b6208d11ef83a6d6cf
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publicationDate 2017-06-02-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber RU-2621343-C1
titleOfInvention 2-[4'-(2",6"-dimethylphenoxy)benzoyl]benzoic acid and the method of preparation of the invention
abstract FIELD: chemistry. n SUBSTANCE: invention relates to 2-[4'-(2",6"-dimethylphenoxy)benzoyl]benzoic acid which can be used as a by-product in the synthesis of polyarylene phthalides with valuable properties. A method for preparing acid I in 77% yield from 2-(4'-fluorobenzoyl) benzoic acid and 2.6-dimethylphenol in the presence of K 2 CO 3 with two-stage heating: first in a mixture of N,N-dimethylacetamide with chlorobenzene until the azeotropic distillation of water and chlorobenzene is completed, then only in N,N-dimethylacetamide. n EFFECT: increased quality of output. n 3 cl, 3 ex
priorityDate 2016-07-11-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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