Predicate |
Object |
assignee |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_a6bf189b45973e2d5070475377187d70 |
classificationCPCAdditional |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C65-40 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C51-367 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C08G61-12 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C08G8-02 |
classificationIPCInventive |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C51-367 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08G61-12 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C65-40 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C08G8-02 |
filingDate |
2016-07-11-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate |
2017-06-02-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor |
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_d870d4f8eed1d1b6208d11ef83a6d6cf http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_9d8677f75cd7d4ef9db44ef3e7c45962 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_9b3ba7efe5e38be7efeb38c1450a3198 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_92c7455a597d09afa5d2a7583bcce4a1 |
publicationDate |
2017-06-02-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber |
RU-2621343-C1 |
titleOfInvention |
2-[4'-(2",6"-dimethylphenoxy)benzoyl]benzoic acid and the method of preparation of the invention |
abstract |
FIELD: chemistry. n SUBSTANCE: invention relates to 2-[4'-(2",6"-dimethylphenoxy)benzoyl]benzoic acid which can be used as a by-product in the synthesis of polyarylene phthalides with valuable properties. A method for preparing acid I in 77% yield from 2-(4'-fluorobenzoyl) benzoic acid and 2.6-dimethylphenol in the presence of K 2 CO 3 with two-stage heating: first in a mixture of N,N-dimethylacetamide with chlorobenzene until the azeotropic distillation of water and chlorobenzene is completed, then only in N,N-dimethylacetamide. n EFFECT: increased quality of output. n 3 cl, 3 ex |
priorityDate |
2016-07-11-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type |
http://data.epo.org/linked-data/def/patent/Publication |