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publicationDate 2017-03-02-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber RU-2612174-C1
titleOfInvention Method of producing ceramic piezomaterials from nano- or ultradisperse powdered oxygen-octahedral type phases
abstract FIELD: chemistry. n SUBSTANCE: invention relates to method of producing ceramic piezomaterials from nano- and ultradisperse powdered oxygen-octahedral type phases containing titanium ions (IV), niobium (V), zirconium (IV), tungsten (VI), zinc (II), nickel (II) and iron (III), cobalt (III) and other p- or d-elements in (B) position. The method of producing ceramic piezomaterials from nano- and / or ultradisperse powdered oxygen-octahedral type phases is characterized by the fact that the nano- and / or ultradisperse powdered oxygen-octahedral type phases are treated with alcoholic or aqueous-alcoholic solution of 1-8 wt % ammonium glycolate (NH 4 HC 2 O 3 ) or ammonium formate (NH 4 COOH), or their mixtures before molding and sintering operation, afterwards the liquid phase is removed and the resulting powder is dried. Press-half-finished product made from the thus treated powder is being sintered for 1.5-3 hours at a temperature from 900 to 1250°C. n EFFECT: invention increases the relative permittivity and piezoelectric modules while maintaining electromechanical coupling coefficients of piezomaterials. n 6 cl, 30 ex, 2 tbl
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