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http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/G01N1-28
filingDate 2014-04-10-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2015-04-10-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_fc628cbadbaba60aef115aba3c02e10a
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publicationDate 2015-04-10-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber RU-2546527-C1
titleOfInvention Method for measuring blood pentachlorophenol by gas chromatography analysis
abstract FIELD: medicine. n SUBSTANCE: blood is sampled, acidified to pH 2-3 with aqueous oxalic acid, extracted in toluene for 5 min; the prepared extract is centrifuged for 60 min at 7,000 rpm, added with sodium sulphate to dewater and acetylated for 3 hours by introducing trifluoroacetic anhydride while stirring continuously in the pyridine medium. The blood sample, toluene, trifluoroacetic anhydride and pyridine are taken in volume ratio 5:2.5:0.2:0.1 respectively. n EFFECT: simplifying the stage of sample preparation and increasing the sensitivity of pentachlorophenol test. n 3 cl, 4 tbl, 1 ex
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