http://rdf.ncbi.nlm.nih.gov/pubchem/patent/RU-2529502-C2
Outgoing Links
Predicate | Object |
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assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_0ec83c1631af3dc0e0aa55046d4d8b75 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D413-04 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D417-06 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D417-04 |
filingDate | 2012-10-26-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2014-09-27-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_d6e920c7ff0f2007ee4df55d7e57183b http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_45e7b9ace9a5182141851a2b96ded46b http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_abe00814fd8d5782e0be57db5daf5818 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_5df4ceab60b4dd0d9f87c22aca4157f7 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_0a995c34657fb9b66919d919ec5a72d6 |
publicationDate | 2014-09-27-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | RU-2529502-C2 |
titleOfInvention | Method of obtaining 3-hetaryl-1,5,3-dithiazepinanes |
abstract | FIELD: chemistry. n SUBSTANCE: invention relates to field of organic chemistry, in particular to method of obtaining 3-hetaryl-1,5,3-dithiazepinanes of general formula (1) , where ; ; ; ; ; ; ; ; , consisting in the following: N 1 ,N 1 ,N 6 ,N 6 -tetramethyl-2,5-dithiahexane-1,6-diamine is subjected to interaction with hetarylamine [2-pyridinamine, 3-pyridinamine, 5-bromo-2-pyridinamine, 5-methyl-2-pyridinamine, 4-pyridinylmethylamine, 5-nitro-1,3-thiazol-2-amine, 6-nitro-1,3-benzothiazol-2-amine, 2-91h-indol-3-yl)-1-ethanamone, 5-methyl-1H-pyrazol-3-amine] in presence of catalyst CuCl 2 in molar ratio N 1 ,N 1 ,N 6 ,N 6 -tetramethyl-2,5-dithiahexane-1,6-diamine:hetarylamine: CuCl 2 =10:10:(0.3-0.7) at temperature 55-65°C and atmospheric pressure in chloroform as solvent for 50-80 minutes. n EFFECT: elaborated is method of obtaining 3-hetaryl-1,5,3-dithiazepinanes, which can be applied as biologically active substances. n 1 tbl, 1 ex |
priorityDate | 2012-10-26-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 57.