http://rdf.ncbi.nlm.nih.gov/pubchem/patent/RU-2499793-C1
Outgoing Links
Predicate | Object |
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assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_ff346a4b8595551f1fdd6153af5a1907 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D211-02 |
filingDate | 2012-08-24-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2013-11-27-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_971b3692fceae7dea7311950fc73cd2b http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_839d5bef9dbd58653ec6e35fc3ad0b0e http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_6a9b8eb289a3e2c64310fb30996902b4 |
publicationDate | 2013-11-27-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | RU-2499793-C1 |
titleOfInvention | Method of producing tertiary amines |
abstract | FIELD: chemistry. n SUBSTANCE: invention relates to a method of producing tertiary amines, particularly a novel method of hydrogenating enamines, which can be used in laboratory conditions and enables to obtain saturated tertiary amines of general formula n , ; n , , . n The method of hydrogenating enamines is characterised by that the enamines used are: 2-methyl-3-(N-piperidino)propene, 2-methyl-3-(N-morpholino)propene, 1-(N-piperidino)cyclohexene-1, 1-(N-morpholino)cyclohexene-1 or 1,4-dicyclohex-1-enylpiperazine, and hydrogenation is carried out with hydrogen at atmospheric pressure in the presence of a catalyst in form of nickel nanoparticles obtained by reducing nickel (II) chloride with sodium borane in situ, in a medium of isopropanol at temperature of 40-70°C for 5-6 hours. n EFFECT: simple and cheap method of producing compounds of the disclosed structural formula. n 1 cl, 5 ex |
priorityDate | 2012-08-24-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 50.