http://rdf.ncbi.nlm.nih.gov/pubchem/patent/RU-2453537-C2

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http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C391-00
filingDate 2007-10-26-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2012-06-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_b1a422a1c1c55254387253ab6c60b714
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_fd99462cb91eea86cc2b43b6c9ddcf76
publicationDate 2012-06-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber RU-2453537-C2
titleOfInvention Method of producing 2-hydroxy-4-methylselenobutyric acid as separate substance or as mixture with sulphur-containing analogue thereof, and use thereof in nutrition, particularly animal nutrition
abstract FIELD: chemistry. n SUBSTANCE: method comprises the following steps: reaction of 3-methylselenopropion aldehyde of formula (I): with an alkali metal cyanide of formula M + CN - , preferably in the presence of an alkali metal bisulphite salt of formula M + HSO 3   - , where M denotes an alkali metal atom, in a polar protic solvent, to obtain 2-hydroxy-4-methylselenobutyronitrile of formula (II): , hydrolysis of the compound of formula (II) in the medium of hot concentrated sulphuric acid, in a polar protic solvent, to obtain the desirable compound of formula (IV): , or hydrolysis of the compound of formula (II) in the medium of hot concentrated sulphuric acid, in a polar protic solvent, to obtain a compound of formula (III): , which can be hydrolysed in the medium of hot concentrated strong acid to obtain a compound of formula (IV). The compound of formula (IV) can be converted to one of its salts after adding a physiologically acceptable base. The invention also discloses a method of preparing a mixture of 2-hydroxy-4-methylselenobutyric acid and 2-hydroxy-4-methylthiobutyric acid and use thereof, 2-hydroxy-4-methylselenobutyronitrile and use thereof, and a dietary composition. n EFFECT: invention simplifies production of 2-hydroxy-4-methylselenobutyric acid. n 17 cl, 7 ex
priorityDate 2006-10-27-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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