http://rdf.ncbi.nlm.nih.gov/pubchem/patent/RU-2423366-C2

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assignee http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_ec5a60ce255cb641b0c16c33bd852230
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07F3-02
filingDate 2009-07-02-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2011-07-10-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_38e51487ed6b68f27826173c0bf682ba
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_3319502ca44e0d04e0253b5991cbf4b7
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_68a0da3222e2576ff0f675c15f6a3380
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_b692ac4554fbd63d91e6c08506db3069
publicationDate 2011-07-10-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber RU-2423366-C2
titleOfInvention Method for synthesis of 2,4,6-triphenylmagnesacyclononane
abstract FIELD: chemistry. n SUBSTANCE: invention relates to a method for synthesis of 2,4,6-triphenylmagnesacyclononane (I) of formula: .The method involves reaction of styrene with magnesacyclopentane in the presence of a zirconocene dichloride Cp 2 ZrCl 2 catalyst. The reaction is carried out in an atmosphere of dry ethylene fed under excess pressure of 0.04 MPa in molar ratio styrene: magnesacyclopentane: Cp 2 ZrCl 2 =(10-20):10:(0.2-0.4), in a tetrahydrofuran solution at 20-22°C for 8-10 hours. n EFFECT: invention enables to obtain 2,4,6-triphenylmagnesacyclononane of the formula given above. n 1 ex, 1 tbl
priorityDate 2009-07-02-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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