http://rdf.ncbi.nlm.nih.gov/pubchem/patent/RU-2423366-C2
Outgoing Links
Predicate | Object |
---|---|
assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_ec5a60ce255cb641b0c16c33bd852230 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07F3-02 |
filingDate | 2009-07-02-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2011-07-10-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_38e51487ed6b68f27826173c0bf682ba http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_3319502ca44e0d04e0253b5991cbf4b7 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_68a0da3222e2576ff0f675c15f6a3380 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_b692ac4554fbd63d91e6c08506db3069 |
publicationDate | 2011-07-10-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | RU-2423366-C2 |
titleOfInvention | Method for synthesis of 2,4,6-triphenylmagnesacyclononane |
abstract | FIELD: chemistry. n SUBSTANCE: invention relates to a method for synthesis of 2,4,6-triphenylmagnesacyclononane (I) of formula: .The method involves reaction of styrene with magnesacyclopentane in the presence of a zirconocene dichloride Cp 2 ZrCl 2 catalyst. The reaction is carried out in an atmosphere of dry ethylene fed under excess pressure of 0.04 MPa in molar ratio styrene: magnesacyclopentane: Cp 2 ZrCl 2 =(10-20):10:(0.2-0.4), in a tetrahydrofuran solution at 20-22°C for 8-10 hours. n EFFECT: invention enables to obtain 2,4,6-triphenylmagnesacyclononane of the formula given above. n 1 ex, 1 tbl |
priorityDate | 2009-07-02-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 38.