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filingDate 2009-09-25-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2011-03-27-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_e93114d0a0a3c0598714a016874a23ea
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publicationDate 2011-03-27-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber RU-2415123-C1
titleOfInvention Method of producing 2-isopropyl-p-xylene and 2,5-diisopropyl-p-xylene
abstract FIELD: chemistry. ^ SUBSTANCE: invention relates to a method of producing 2-isopropyl-p-xylene and 2,5-diisopropyl-p-xylene through alkylation of p-xylene with propylene in liquid phase, characterised by that p-xylene undergoes alkylation at temperature 70-90C, and at the first step alkylation is carried out in the presence of a AlCl3 catalyst until achieving 40-90% conversion of the initial hydrocarbon and accumulation of 30-50% mono-isopropyl-p-xylene in the alkylate. Further, 5-mono-isopropyl-p-xylene undergoes alkylation at the second step in the presence of AlCl2H2PO4 such that, after achieving total content of isomers 2,5-, 2,3-, 2,6-di-isopropyl-p-xylene of 30-50% in the alkylate, supply of propylene is cut and the obtained alkylate is held at temperature 70-90C for 2-6 hours until achieving at least 95% concentration of 2,5-di-isopropyl-p-xylene and then extracting the end product using known techniques. ^ EFFECT: engineering solution simplifies production of mono-isopropyl-p-xylene and 2,5-diisopropyl-p-xylene and increases output of end products. ^ 1 cl, 7 ex, 1 tbl, 1 dwg
priorityDate 2009-09-25-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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