http://rdf.ncbi.nlm.nih.gov/pubchem/patent/RU-2268874-C2
Outgoing Links
Predicate | Object |
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classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07F15-02 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C53-10 |
filingDate | 2004-03-22-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 2006-01-27-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_9e1d6ec53cf0aa395922e0e8a04579de http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_107e720a5f448c6d032685d821663bb4 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_49b8513f54c8db51cd6b7c3855a1b0c2 |
publicationDate | 2006-01-27-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | RU-2268874-C2 |
titleOfInvention | Basic ferric acetate preparation method |
abstract | FIELD: industrial inorganic synthesis. n SUBSTANCE: implementation of the method comprises contacting iron in the form of iron powder or iron sidewall adjacent to a body with glacial acetic acid and air oxygen at 17-25°C and vigorous stirring effected by high-speed blade-type mechanical stirrer. Initial acetic acid-to-iron molar ratio is (224÷274):100. Acetic anhydride additive is preferably introduced in amount of 2% based on the initial concentration of acetic acid. When concentration of ferric salt in the mixture reaches 2.70-3.51 mole/kg, stirring is stopped and heavy unreacted iron particles are allowed to settle/ Major mass of product suspension is filtered off and thus obtained basic ferric acetate precipitate is dried. Filtrate, which is saturated acetic acid solution of basic ferric acetate, is returned into reactor to be reprocessed. Yield of desired product achieves 99.2-99.3%. n EFFECT: simplified process and improved economical efficiency due to utilization of inexpensive raw material and accessible oxidant. n 2 ex |
priorityDate | 2004-03-22-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 31.