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filingDate 2004-03-16-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2005-12-10-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_26b2c0feeb78285c9ad292f6b14b6101
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publicationDate 2005-12-10-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber RU-2265578-C1
titleOfInvention Method of production of vanadium pentafluoride
abstract FIELD: production of highly volatile higher fluorides of multi-valent metals. n SUBSTANCE: proposed method includes fluorination of wastes: chips, fragments, substandard vanadium articles by element fluorine, distillation of vanadium pentafluoride thus formed and its condensation. Fluorination is performed at two stages: first fluorine is admitted to reactor to excessive pressure of 1.5-2.0 kPa and vanadium batch is held for an hour at temperature of 40-60°C; then reactor is heated to initial temperature of 180-200°C and chips are fluorinated by commercial fluorine containing 92-94 vol-% of fluorine, 4-6 vol-% of hydrogen fluoride; the remainder being inert admixtures. Vanadium pentafluoride thus formed is condensed at temperature of (-25)-(-30)°C into bottles-condensers which are held under rarefaction of 2.0-3.0 kPa for 2 h at temperature of (-25)-(-30)°C. n EFFECT: low cost of product; increased yield of finished product. n 2 ex
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type http://data.epo.org/linked-data/def/patent/Publication

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Total number of triples: 36.