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classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07F5-06
filingDate 1996-02-22-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2000-09-10-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_d2e9e219db857fdfaafaad6a67729322
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_e1219d99abb54869165bc0660339fe75
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publicationDate 2000-09-10-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber RU-2155768-C2
titleOfInvention Method of preparing 1,2-bis/(dialkylamine)aluma/cis-1,2- diphenyl (alkyl)ethylenes
abstract FIELD: metal and fine organic synthesis. SUBSTANCE: method comprises reacting bis(dialkylamine) aluminium chlorides wherein R′ is Et, n-C 6 H 13 with disubstituted acetylene of formula: R-≡-R wherein R is Ph, n-C 3 H 7 , n-C 4 H 9 and metallic magnesium at molar ratio of (25-35): 10:(10-14) in the presence of titanocene dichloride ((Cp 2 TiCl 2 )) in amount of 2-5 mole % with respect to disubstituted acetylene in argon atmosphere under normal conditions in hydrofuran during stirring operation for 8- 12 hours. The resulting new compounds are used as catalyst complex components in processes of polymerization and oligomerization of olefin and diene hydrocarbons and also in metallic and fine organic synthesis. EFFECT: more efficient preparation method. 1 ex, 1 tbl
priorityDate 1996-02-22-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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