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filingDate 1996-07-31-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 1998-01-27-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_38ae410398759afcdb6483f48f34b2a5
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publicationDate 1998-01-27-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber RU-2103372-C1
titleOfInvention Method of preparing titanium tanning agents for skin
abstract FIELD: leather industry. SUBSTANCE: initial titanyl sulfate solution with much insoluble precipitate is prepared, allowed to stand at 35-39 C to form clarified solution with titanium concentration 38 to 44.5 g/l. Upper layer is separated and enriched in titanyl sulfate to 80-140 g/l titanium, 180-340 g/l sulfate ion, and not higher than 65 g/l chloride ion. Solution is then agitated, cooled, and desalting by ammonium sulfatitytanyl is effected by way of adding solid ammonium sulfate in two steps: first 30-40% ammonium sulfate of its total amount is added at the rate 0.22-0.27 kg/s and then remaining 70-60% with the rate 0.06-0.07 kg/s. Afterwards, crystallization, suspension filtration, and precipitate treatment are performed. EFFECT: optimized preparation procedure. 2 tbl
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