http://rdf.ncbi.nlm.nih.gov/pubchem/patent/RU-2103249-C1
Outgoing Links
Predicate | Object |
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assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_0b84fb79483de2f5d1cfd4844937be32 http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_94b9809d6de263b1c6572595e0d05852 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C2-36 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C11-12 |
filingDate | 1995-01-25-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 1998-01-27-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_c7b0b34263fb425d08360896ca0b178d http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_b2ed47e68b421954a38d9e3fcb9c3355 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_a533e268bbd3afb1d45662305e1727ee http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_a6e9c8ccc41a975745b03fab1fb6d228 |
publicationDate | 1998-01-27-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | RU-2103249-C1 |
titleOfInvention | Method for producing 2-alkyl substituted 1,3-dienes |
abstract | FIELD: petrochemistry, namely, origin materials for production of aromatic principles, attractants, polymer materials, paints, varnish and other. SUBSTANCE: 2-alkyl substituted 1,3-dienes have common formula where R is C 4 H 9 , C 6 H 13 , C 9 H 19 are prepared by consequent mixing of solution of triethylene aluminium in aliphatic solvents Cp 2 Z 1 -Cl 2 and with α-olefin, their molar ratio being (10-12):(0.2-0.4):10. The process is followed by mixing at room temperature within 8 h, then at temperature about (-5) C catalyst is added. Said catalyst is prepared by mixing Ni(acai) 2 , Ph 3 P and i-Bu 2 AkH followed by adding allyl acetate at their molar ratio (0.3-0.5): (1.2-2.0):(2.4-4.0):(30-36) respectively, the process takes place in aliphatic solvents by mixing of reaction mixture at room temperature within 8-12 h. Yield of 2-alkyl substituted 1,3-dienes is 60-84 %. EFFECT: improved quality of desired product. 1 tbl |
priorityDate | 1995-01-25-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 57.