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filingDate 1994-06-29-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 1997-11-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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publicationDate 1997-11-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber RU-2096425-C1
titleOfInvention Preparation of butadiene-styrene rubbers
abstract FIELD: synthetic rubber industry, more particularly preparation of butyl-styrene rubbers. SUBSTANCE: butyl-styrene rubbers are prepared by copolymerization of butadiene with styrene in hydrocarbon solvent in several in series connected reactors at 45-90 C in the presence of organolithium initiator. Copolymerization is carried out in the presence of cocatalyst additive of formula: C 6 H 2 (R 1 )(R 2 )(R 3 )(OK), wherein R 1 , R 2 , R 3 are H or at cocatalyst to organolithium compound molar ratio of from 0.04: 1 to 0.2:1, respectively. In this case, cocatalyst is added in amount of 0.01 to 0.5 wt % based on total amount of comonomers. Fatty acids of formula RCOOH, wherein R is C 12 -C 20 alkyl, are added together with cocatalyst into the last reactor. Fatty acids are added in amount of 0.005 to 0.8 wt % based on total amount of comonomers. EFFECT: more efficient preparation method. 2 tbl
priorityDate 1994-06-29-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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