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classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C25-13
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C17-12
filingDate 1995-05-24-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 1997-07-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_629adcf95712d8d1e149ecbad852afd8
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_114a6839edad26480bbbe6ba28e89e69
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publicationDate 1997-07-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber RU-2084437-C1
titleOfInvention Method of synthesis of hexafluorobenzene or its mono- or disubstituted derivatives
abstract FIELD: chemical technology. SUBSTANCE: invention relates to chemical technology of polyfluoroarenes, in part, synthesis of hexafluorobenzene or its mono- or disubstituted derivatives of the formula C 6 F 4 -XY where: X - F, Cl, H, CF 3 , CCl 3 ; Y - F, CN, H, Cl, CF 3 , CCl 3 . These derivatives were synthesized by chlorine substitution in the corresponding polychloroarenes with potassium fluorofluoride without solvent at heating to 150-250 C in the presence of catalytic system quaternary phosphonium salt/water at mole ratio of components = (1:0.5)-(1:50) and mole ratio potassium fluoride and quaternary phosphonium salt = (200:1)-(10:1). The yield of the end product is up to 98.7%. Synthesized compounds were used for synthesis of dyes, drugs, monomers. EFFECT: improved method of synthesis, increased yield. 5 cl
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priorityDate 1995-05-24-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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