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filingDate 1992-01-09-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 1996-02-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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publicationDate 1996-02-20-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber RU-2054430-C1
titleOfInvention 4-trimethylsiloxymethylphosphinyl-2-trimethylsiloxy-2-cyanobutiro nitrile as intermediate product in synthesis of 4-methylhydroxyphosphinyl-2-aminobtanoic acid having herbicide activity and method for its production
abstract FIELD: organic chemistry. SUBSTANCE: desired product has formula CH 3 P(O)[OSi(CH 3 ) 3 ]CH 2 CH 2 C(CN) 2 [OSi(CH 3 ) 3 , its essential formula being C 12 H 25 N 2 O 3 Si 2 P. Compound having formula CH 3 P(O) /bond O-C(O)-CH 2 -CH 2 / bond with phosphorous/ is used as reagent 1. Compound having formula (CH 3 ) 3 SiCN is used as reagent 2. Reaction is carried out at 60-70 C within 6-7 h in the presence of titanium tetrachloride, molar ratio of reagents being 1:(2-4): 0.01. Said reaction takes place in chloroform medium. Desired product is prepared as oil at yield 100 %. EFFECT: improves quality of desired product, improves efficiency of method. 4 cl, 2 tbl
priorityDate 1992-01-09-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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