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publicationDate 1995-11-10-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber RU-2047592-C1
titleOfInvention Process for preparing calcium salt of phenylpyroracemic acid
abstract FIELD: organic chemistry. SUBSTANCE: the product: pyroracemic acid of the empirical formula: C 18 H 14 O 6 Ca.. The content of impurities is 5-6% the yield is 70-75% Reagent 1: benzyl chloride. Reagent 2: carbon oxide. Reaction conditions: in the aqueous alcoholic medium at 35-45 C and at a CO pressure of 1-5 atm in the presence of calcium oxide or hydroxide and a catalyst such as a cobalt carbonyl compound at a cobalt concentration of 1.5-4.0% EFFECT: more efficient preparation process. 1 tbl
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