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http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D403-14
filingDate 1991-06-28-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 1994-12-15-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_16b573c3fe34cab3e75312122a63b924
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publicationDate 1994-12-15-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber RU-2024518-C1
titleOfInvention Method of synthesis of 1- (2,4,6 -trichlorophenyl) -3- [2- chloro -5 -(octadecenylsuccineimi- do)-anilino] -4- (1- decyl- 3,5- dimethylpyrazole -4-ylazo)- pyrazol - ine -5- one
abstract FIELD: organic chemistry. SUBSTANCE: product - 1-(2,4,6- trichlorophenyl) -3- [2-chloro -5 -(octadecenyl succineimi - do) -anilino] -4- (1- decyl -3,5- dimethylpyrazole -4-ylazo)- pyrazol - ine -5-one of the formula (image), empirical formula is БФ С 52 H 72 N 8 Cl 4 O 3 , m. p. is 90-92 C, yield is 40% . Reagent 1: 1-decyl-3,5-dimethyl-4-aminopyrazole. Reagent 2: NaNO 2 . Reaction conditions: in water in the presence of HCl at 0-2 C. Reagent 3: 1-(2,4,6-trichlorophenyl)-3-[2-chloro-5-octadecenylsuccineimi- do)-phenylamino]-pyrazoline-5-one. Reaction conditions: in pyridine, at 10-15 C. Product is used in negative photographic materials. EFFECT: improved method of synthesis. 2 tbl
priorityDate 1991-06-28-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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