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classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C327-06
filingDate 1991-01-29-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 1994-10-15-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_d84ea51723ca140db94b19de592363cd
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publicationDate 1994-10-15-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber RU-2021261-C1
titleOfInvention Method of synthesis of difluorothioacetylfluoride
abstract FIELD: organic chemistry. SUBSTANCE: product - difluorothioacetylfluoride - HCF 2 CF=S, empirical formula is C 2 HF 3 S, b. p. is 14-16 C, yield is 66-71% . Reagent 1: benzyl-1,1,2,2-tetrafluoroethylsulfide. Reagent 2: phosphoric anhydride taken at 1.5-2-fold molar excess. Reaction conditions: heating up to 150-180 C. EFFECT: improved method of synthesis.
priorityDate 1991-01-29-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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