http://rdf.ncbi.nlm.nih.gov/pubchem/patent/RU-2013152027-A
Outgoing Links
Predicate | Object |
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classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C319-14 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C323-37 |
filingDate | 2013-11-21-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2015-05-27-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | RU-2013152027-A |
titleOfInvention | METHOD FOR PRODUCING N, N, N-THREE [(Phenyl (Benzyl) Sulfanyl) Methyl] AMINES |
abstract | The method of producing N, N, N-tri [(phenyl (benzyl) sulfanyl) methyl] amines of the general formula (1): where R = Ph, Bn, by reacting phenyl (benzyl) thiols of the general formula R-SH [R = above ], with hexamethylenetetramine taken in the stoichiometric ratio of thiol: hexamethylenetetramine = 60:10, characterized in that the reaction is carried out in the presence of a catalyst of crystalline hydrate of samarium nitrate supported on γ-AlO, with the content of the catalyst Sm (NO) · 6 · HO / γ- AlO in a reaction mass of 0.03-0.07 wt.% With respect to hexamethylenetetramine in chloroform as a solvent at a temperature ur 50-70 ° C and atmospheric pressure for 3-5 hours |
priorityDate | 2013-11-21-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 20.