http://rdf.ncbi.nlm.nih.gov/pubchem/patent/RU-2012154465-A
Outgoing Links
Predicate | Object |
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classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D417-00 |
filingDate | 2012-12-14-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2014-06-20-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | RU-2012154465-A |
titleOfInvention | METHOD FOR SELECTIVE OBTAINING 3,3 '- [BIS- (1,4-PHENYLENE)] BIS-1,5,3-Dithiazepinanes |
abstract | The method of selective preparation of 3,3 '- [bis- (1,4-phenylene)] bis-1,5,3-dithiazepinans of the general formula (1): R = 4-CH-CH-CH-4,4-CH- O-CH-4,4-HCOCH-CHOCH-4, characterized in that diphenylenediamines (diaminodiphenylmethane, diaminodiphenyl oxide, dimethoxybenzidine) are reacted with 1-oxa-3,6-dithiacycloheptane in the presence of a Sm (NO) · 6HO catalyst in an argon atmosphere at a diphenylenediamine: 1-oxa-3,6-dithiacycloheptane molar ratio: Sm (NO) · 6HO = 1: 2: (0.03-0.07) at a temperature of ~ 20 ° C in an ethanol-chloroform solvent system for 2.5-3.5 h. |
priorityDate | 2012-12-14-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 17.