http://rdf.ncbi.nlm.nih.gov/pubchem/patent/RU-2012150739-A
Outgoing Links
Predicate | Object |
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classificationCPCAdditional | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C2601-10 |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/B01J31-2295 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C2-54 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C2-861 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C2-868 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07F17-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C17-32 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C1-326 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C41-30 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C2-86 |
filingDate | 2011-04-05-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2014-06-10-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | RU-2012150739-A |
titleOfInvention | SYNTHESIS OF ALKYLCYCLOPENTADIENE COMPOUNDS |
abstract | 1. The method of synthesis of at least one alkylcyclopentadiene compound, which includes alkylcyclopentadiene and its substituted alkyl derivatives, comprising: contacting at least one cyclopentadienyl anion source comprising at least one reagent selected from the group consisting of Grignard cyclopentadienyl reagent, sodium cyclopentadienyl, lithium cyclopentadienyl, potassium cyclopentadienyl and any combination of the above, and at least one source of an alkyl group, including at least shey least one reactant selected from the group consisting of alkyl halides and alkyl sulfonate, for a period lasting from 4 to 7 hours at a temperature of from 50 to 65 ° C, to yield at least one compound alkiltsiklopentadienovogo; extraction of the alkyl cyclopentadiene compound with a hydrocarbon solvent, wherein the molar ratio of the source of the alkyl group to the source of the cyclopentadienyl anion is from 0.5: 1 to 0.9: 1.2. The method of claim 1, wherein the cyclopentadienyl anion source comprises Grignard cyclopentadienyl reagent. The method according to claim 1 or 2, in which the molar ratio of the source of the alkyl group to the source of the cyclopentadienyl anion is from 0.5: 1 to 0.8: 1.4. The method according to claim 1 or 2, in which the molar ratio of the source of the alkyl group to the source of the cyclopentadienyl anion is 0.75: 1.5. The method according to claim 1 or 2, wherein the alkyl cyclopentadiene compound comprises a Acryl group. The method according to claim 1 or 2, wherein the alkyl cyclopentadiene compound comprises an alkyl group substituted with one or more heteroatoms or one |
priorityDate | 2010-04-28-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 47.