http://rdf.ncbi.nlm.nih.gov/pubchem/patent/RU-1816754-C

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http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C41-14
filingDate 1990-11-21-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 1993-05-23-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_ce3a54873cfe42f8eece15eb046cf868
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publicationDate 1993-05-23-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber RU-1816754-C
titleOfInvention Method of synthesis of alcohol or phenol difluoromethyl esters
abstract Usage: As components of liquid crystal compositions for electro-optical devices. Essence: an improved method for the preparation of difluoromethyl ethers or phenols of the general formula R — OCHPr, where R is lower alkyl, cyclohexyl. Alk - SvNyu - CeHto - CHa, Alk - SvZhO - SvN4CH2. RI - C “Nude. where Ri is Alk. Alk - SvN, R2 - CeN ", where: R2 - CN. Alk, Alk - SeN Alk - CBH4. Afk - SbNu - SvZhO, where Alk - SzNU, CsHn. Reagent 1: chlorodifluoromethane. Reagent 2: corresponding alcohol, Reaction conditions: two-phase system, temperature 20-60 °; C, catalyst: a mixture of quaternary ammonium hydroxide of the formula (8h) OH, where Rs SMz, C4Y9, go and try tritylbenzylammonium with three trimethylbenzylammonium chloride in a molar ratio of alcohol: quaternary ammonium hydroxide or trichloroethyltrimethylthenethyltriethylthenethylthenethylthenethylthenethylthenethylthenethylthenethisethyl : (0.6-1.3): {0.0002-0.002), in an organic solvent. The yield of the target product to 100%. New phycols of iclohexanol are obtained. 1 tab. yo yo
isCitedBy http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-9150491-B2
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priorityDate 1990-11-21-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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