http://rdf.ncbi.nlm.nih.gov/pubchem/patent/RU-1806138-C
Outgoing Links
Predicate | Object |
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assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_d61c1c5b16f752b909935d3d1809f0e1 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D263-57 |
filingDate | 1991-03-29-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 1993-03-30-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_bbce2867658246eeacf9d5abf786ed5e http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_d514b022a2414d970f0deba1eaa154b4 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_ff03eb66fa7461e8383ced0753e9f6c2 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_3ae1be2ca9dd0b37c58f476e29d6548e http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_4667c353b0798f4e87a6954562f0176b |
publicationDate | 1993-03-30-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | RU-1806138-C |
titleOfInvention | Method for production 2-phenylbenzoxazole |
abstract | Usage: as a phyto-protective drug. SUMMARY OF THE INVENTION: The product is 2-phenylbenzoxazole. BF SiNeMO, yield 77.9%, etc. 101.5-102 ° C. Reagent 1: o-aminophenol. Reagent 2: benzoic acid. Reaction conditions: in the presence of boric acid in xylene medium with the addition of montmorillonite type colloidal clays with a mass ratio of o-aminophenol-clay 1: 0.1-0.5. The resulting mass is filtered, xylene is distilled off, the crude product is crystallized in isopropyl alcohol. And treated with activated carbon in isopropyl alcohol at boiling. 1 tab. 1 ill. (In order to utilize production waste. The goal is achieved in that the condensation of o-amino phenol with benzoic acid in the presence of boric acid in xylene is carried out with the addition of montmorillonite-type colloidal clays with a mass ratio of o-aminophenol-clay 1: 0,1-10, 5, the resulting mass is filtered, xylene is distilled off, the crude product is isolated by crystallization in isopropyl alcohol and it is treated activated00 § CO 00 with |
priorityDate | 1991-03-29-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 32.