http://rdf.ncbi.nlm.nih.gov/pubchem/patent/RU-1707942-C
Outgoing Links
Predicate | Object |
---|---|
assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_7aa119638bc9e1af9a647a52b414b650 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C205-15 |
filingDate | 1988-03-16-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
grantDate | 1995-08-27-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_7ed3f9eeb42234cc88fd66883ca6260c http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_f3ba8ae642f15e2bbfaf22d5431598cd http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_f34af26a2b0c5b237228ebfd4f71eed4 |
publicationDate | 1995-08-27-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | RU-1707942-C |
titleOfInvention | Method for production of potassium salt of 2,2-dinitroethanol |
abstract | FIELD: organic chemistry. SUBSTANCE: method involves treatment of trinitromethane by aqueous solution of formaldehyde and of copper sulfate pentahydrate. The process is carried out at 100-101 C within 9.5-10.0 h. It is followed by cooling reaction mass to 0-5 C and by adding aqueous solution of KOH, molar ratio of reagents is 1:11.7-12.7:0.02-0.28:2.0-2.5 respectively. Desired product is isolated by adding acetone and by washing with it. Desired product having essential formula C 2 H 3 N 2 O 5 K. is prepared by yield 76 its melting point being 130-132 C. EFFECT: simplifies the method, increases its safety. |
priorityDate | 1988-03-16-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 33.