http://rdf.ncbi.nlm.nih.gov/pubchem/patent/PL-423818-A1

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filingDate 2017-12-11-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_56315b630718ade2f01960c8021876b6
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publicationDate 2019-06-17-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber PL-423818-A1
titleOfInvention A method of obtaining a mixture of transition metal oxides in the form of an airgel
abstract The subject of the application is a method of obtaining a mixture of transition metal oxides in the form of an airgel, which is characterized in that the transition metal salts are manganese (II) tetrahydrate and nickel (II) chloride hexahydrate and / or cobalt (II) chloride hexahydrate. which are dissolved in methanol and / or ethanol, but the total content of transition metal salts used in the resulting salt solution in the solvent is kept between 13% and 25% by weight. The gelation reaction is then carried out in such a way that from 100 g of the obtained salt solution in solvent from 30 g to 59 g of epoxide in the form of butyl glycol ether is added and the mixture thus obtained is left in an atmosphere with an oxygen content of less than 3% by weight at a temperature of from 18 ° C to 32 ° C until gelation. Then, while still maintaining the conditions with reduced oxygen content below 3% by weight, the obtained gel is dried under supercritical conditions with the participation of alcohol until obtaining a mixture of transition metal oxides with an airgel structure.
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