http://rdf.ncbi.nlm.nih.gov/pubchem/patent/PL-231372-B1

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assignee http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_0a940b4583a4cbe5a46f3ac147727134
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D311-92
filingDate 2016-01-19-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_607b4745fef7c88f88da913ca3b87c3f
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_7bd82d47d2aa180cec322c91733f0de9
publicationDate 2019-02-28-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber PL-231372-B1
titleOfInvention The method of obtaining β-lapachone
abstract The subject of the application is a method for obtaining ß-lapachone, consisting in the cyclization of lapachol in an acid medium, and then isolating crude ß-lapachone from the reaction medium and its crystallization, characterized in that lapachol is subjected to a cyclization reaction in a methanesulfonic acid medium, and after After cyclization, the crude β-lapachone is isolated from the reaction mixture by cooling it and diluting it with water, after which the crude β-lapachone precipitate is crystallized from nitromethane and dried.
priorityDate 2016-01-19-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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