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filingDate 1998-04-10-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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publicationDate 2008-03-31-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber PL-197291-B1
titleOfInvention Method for obtaining dimethyl isophthalate and dimethyl terephthalate from the waste fraction from the dimethyl terephthalate production process
abstract The method of obtaining dimethyl isophthalate and dimethyl terephthalate from the waste fraction from the processnfor the production of dimethyl terephthalate, characterized in that the waste fraction from the production of dimethyl terephthalatencontaining dimethyl terephthalate and dimethyl isophthalate is mixed while hot with the aqueous solutionnsodium metabisulphite with a concentration depending on the content of methyl p-formylbenzoate in the wastenfraction so that the stoichiometric ratio of methyl p-formylbenzoate to sodium metabisulfitenwere greater than 1: 2, it is cooled and centrifuged, then the waste fraction is crystallized from the solutionndimethyl isophthalate in methanol, saturated at the final crystallization temperature wherenthe crystallization is carried out such that the temperature of the crystallized solution is lowered by 5-10 ° C belownthe final crystallization temperature, then the solution is heated to the final crystallization temperature,nand the precipitate containing dimethyl terephthalate and dimethyl isophthalate is centrifuged.
priorityDate 1998-04-10-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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