http://rdf.ncbi.nlm.nih.gov/pubchem/patent/PL-157819-B1
Outgoing Links
Predicate | Object |
---|---|
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07H- http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07J19-00 |
filingDate | 1988-07-14-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 1992-07-31-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | PL-157819-B1 |
titleOfInvention | Method of obtaining pure beta-methyldigoxine |
abstract | A method of obtaining pure ß-methyldigoxin by methylating digoxin in a solution of dimethylformamide and a neutral solvent in the presence of barium, aluminum or strontium hydroxide, and then separation on a chromatographic column in the SiC2 / hydrogen chloride system and lower alcohol, characterized in that the reaction solution is washed away from the reaction solution. water, dimethylformamide, and then the solution in a neutral solvent, which is the medium of the reaction, is dosed onto a chromatography column characterized in that a saturated water mobile phase is passed through, the alcohol content of which changes abruptly during the separation cycle. PL PL PL |
priorityDate | 1988-07-14-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 69.