http://rdf.ncbi.nlm.nih.gov/pubchem/patent/MX-2018016293-A

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filingDate 2018-12-13-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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publicationDate 2020-08-17-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber MX-2018016293-A
titleOfInvention PROCESS FOR OBTAINING MICROPARTICLES FROM ETHANOL EXTRACT FROM HABANERO CHILI (CAPSICUM CHINENSE).
abstract The present invention refers to an improved process for obtaining microparticles of ethanolic extract of habanero chili with a greater retention of capsaicin and capsanthin, under the following conditions. Obtaining an ethanolic extract by means of a solid-liquid extraction in multiple stages by countercurrent batch, incorporating in the semi-continuous regime from 23 to 27 kg of solvent for each kg of crushed dried habanero pepper originally fed. Each stage is operated for 120 min, at a temperature of 55 °C, with an agitation of 0.45 g. Obtaining the microparticles by using the supercritical CO2 precipitation method as an antisolvent, using polyvinylpyridone as an encapsulating material at a concentration of 65 - 70% with respect to the total solids of the feed, using the following pressure conditions of 13.5 - 14.5 MPa, temperature of 42 - 48 °C and a flow of 22 - 28 g/min; obtaining microparticles with a size of 17.27 ± 0.85 µm (d50) and a concentration of total capsaicinoids (capsaicin + dihydrocapsaicin) of 101.30 ± 4.74 mg/g of product. This product obtained has various applications in the food, pharmaceutical, cosmetic, and tobacco industries, among others. The process is integrated by 3 steps executed continuously, (a) solid-liquid extraction in multiple stages by countercurrent batch (b) consists in the preparation of the feed mixture to the precipitation system, (c) the solids present in Habanero pepper extract (habanero pepper extractable solids and PVP) are precipitated with supercritical CO2 extract (anti-solvent) within a Thar Technologies SAS 200 precipitation system. The habanero pepper extract was fed without prior evaporation of ethanol.
priorityDate 2018-12-13-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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Total number of triples: 28.