http://rdf.ncbi.nlm.nih.gov/pubchem/patent/KR-960029329-A
Outgoing Links
Predicate | Object |
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classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D317-60 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D317-64 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D317-54 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/A61K31-36 |
filingDate | 1995-01-24-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 1996-08-17-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | KR-960029329-A |
titleOfInvention | Improved Process for the Preparation of Methyl 3-methoxy-4,5-methylenedioxybenzoate |
abstract | The present invention provides the preparation of dimethyl 4,4'-dimethoxy-5,6,5 ', 6'-dimethylenedioxybiphenyl-2,2'-dicarboxylate (DDB) which is usefully used as an intercalating agent. A modified process for the preparation of methyl 3-methoxy-4.5-methylenedioxybenzoate of the general formula (IV) below, which is used as an intermediate, relates to methyl 3-methoxy-4.5-dihydride of the general formula (III) In preparing methylene 3-methoxy-4.5-methylenedioxybenzoate of the general formula (IV), the reaction of methylene dichloride with oxybenzoate is carried out with cesium carbonate in the presence of dimethylformamide. Provide a method.n n n → n n n (Ⅲ) (Ⅳ)n n n The method of the present invention is superior in yield to the conventional method, and the reaction is carried out simply and quickly. |
priorityDate | 1995-01-24-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 26.