http://rdf.ncbi.nlm.nih.gov/pubchem/patent/KR-20200118765-A
Outgoing Links
Predicate | Object |
---|---|
assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_33c922e05f6133b7d72dbb849d77487d |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/G01N33-44 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/H01J49-0009 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/H01J49-0036 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/G01N1-2813 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/G01N27-64 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/H01J49-0418 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/H01J49-164 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/G01N33-442 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/G01N33-44 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/G01N27-64 |
filingDate | 2020-04-07-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_2743f2a4e37a79af5a9d0d39bc720e06 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_69ad7eb94ed5481e3c9084c3435f1596 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_c386185a7b6e2626bc777fa39de1856e http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_f773ee5a61355c2bc32425b6aa32d257 |
publicationDate | 2020-10-16-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | KR-20200118765-A |
titleOfInvention | Method for relative quantitatification of polymers using maldi mass spectrometry |
abstract | The present invention comprises the steps of: (S1) electrospraying a solution containing a polymer sample, a single molecule internal standard material, and a matrix through a mask to prepare a plurality of polymer samples having a thickness deviation of 30% or less for each concentration of the polymer sample; (S2) irradiating a laser to each of the plurality of polymer specimens to obtain a MALDI mass spectrum, and calculating a signal intensity ratio of the polymer sample and the single molecule internal standard material from the peak result of the spectrum; And (S3) it provides a relative quantitative analysis method of a polymer using MALDI mass spectrometry comprising the step of creating a quantitative calibration line by showing the calculated signal intensity ratio by concentration of the polymer sample. According to the present invention, a homogeneous polymer specimen having a small thickness deviation is prepared by an electrospray method using a mask to perform MALDI mass spectrometry, and at this time, the MALDI mass spectrum with reduced peak overlap due to the use of a monomolecular compound as an internal standard material. Can be obtained, from which more accurate relative quantitative analysis of the polymer can be performed. |
priorityDate | 2019-04-08-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 44.