http://rdf.ncbi.nlm.nih.gov/pubchem/patent/KR-20200109404-A

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classificationCPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C23-18
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http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C17-392
filingDate 2019-03-12-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_d96f7d1d80b99b91071da25b5176f8c5
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_f81ff76ffa19395558b9a882543b0cef
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publicationDate 2020-09-23-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber KR-20200109404-A
titleOfInvention Manufacturing method for high purity, high yield 1,1,2,2,9,9,10,10-octafluoro [2.2] paracyclophane (AF4) using cooling recrystallization separation technique
abstract The present invention utilizes the difference in the solubility of AF4 according to the type of solvent, and uses a cooling recrystallization separation technology capable of removing impurities through cooling recrystallization during the manufacturing process of AF4, a monomer of parylene HT. ,1,2,2,9,9,10,10-octafluoro[2.2]paracyclophane (AF4). The present invention is a method for purifying AF4 (1,1,2,2,9,9,10,10-octafluoro[2.2]paracyclophane), comprising: dissolving AF4 and impurities in a solvent; And cooling the solvent, wherein a difference in solubility (g/100g solvent) of AF4 in the solvent according to a temperature change in the cooling step is 70% or more.
priorityDate 2019-03-12-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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