http://rdf.ncbi.nlm.nih.gov/pubchem/patent/KR-20140120170-A

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filingDate 2013-04-02-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_3732092ac41214f2452fc17621ec13f1
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publicationDate 2014-10-13-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber KR-20140120170-A
titleOfInvention Method for manufacturing ceramic powder for protective layer of metallic seperator of solid oxide fuel cell and protective layer thereof
abstract According to an aspect of the present invention, there is provided a method for preparing a ceramic powder for a protective layer of a metal oxide separator of a solid oxide fuel cell, comprising the steps of: preparing a sol by reacting a metal nitrate with a chelating agent; Heating the sol solution to prepare a gel; Continuously heating the gel to pyrolyze; Heat-treating the pyrolyzed gel at a high temperature while bringing the pyrolyzed gel into contact with dry air in a furnace to form a powder; And cooling the heat-treated powder in a furnace. The ceramic powder for a protective layer of a solid oxide fuel cell metal separator according to another embodiment of the present invention may be in the form of a spinel, and may have a mixture of cubic and tetragonal phases. According to still another aspect of the present invention, there is provided a method for manufacturing a protective film for a solid oxide fuel cell metal separator, comprising: preparing a sol by reacting a metal nitrate as a starting material with a chelating agent; The gel is continuously heated and pyrolyzed, and the pyrolyzed gel is heat-treated at a high temperature while being in contact with dry air in a furnace to form a powder, and the heat-treated powder is heated in a furnace ) To prepare a ceramic powder prepared by cooling it; Mixing the ceramic powder with a binder, a surfactant, a dispersant, and a solvent to prepare a slurry; Coating the slurry on a metal separator surface; Drying the slurry coated on the surface of the metal separator at room temperature; Heat treating the coated metal separator at a high temperature while contacting the coated metal separator with dry nitrogen; Heat treating the coated metal separator at a high temperature while contacting the coated metal separator with dry hydrogen; Heat treating the coated metal separator at a high temperature while contacting the coated metal separator with dry oxygen; And cooling in a furnace after the heat treatment step.
isCitedBy http://rdf.ncbi.nlm.nih.gov/pubchem/patent/KR-20200099784-A
http://rdf.ncbi.nlm.nih.gov/pubchem/patent/US-11563220-B2
http://rdf.ncbi.nlm.nih.gov/pubchem/patent/WO-2019245298-A1
http://rdf.ncbi.nlm.nih.gov/pubchem/patent/KR-20190044546-A
priorityDate 2013-04-02-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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