http://rdf.ncbi.nlm.nih.gov/pubchem/patent/KR-20140099863-A
Outgoing Links
Predicate | Object |
---|---|
assignee | http://rdf.ncbi.nlm.nih.gov/pubchem/patentassignee/MD5_4f51818f4238424fa5e29f12c21502ca |
classificationCPCAdditional | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/Y02P20-582 |
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C23C16-18 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C23C16-301 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C23C16-00 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07F5-00 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C23C16-18 http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07F5-00 |
filingDate | 2012-11-28-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
inventor | http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_406359d2c2dfbc4ff4bb54d8427bb502 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_45d8a83615c2071625e35e4e38401d9d http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_886ca86655480f4e82c9c64ab030017a http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_a59676f94d54dd7e7a94ebf98031fc2a http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_e8acac6beeee7f3643c8237244777905 http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_cb6a7987476b6ad9fb884dd2b751d25b |
publicationDate | 2014-08-13-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | KR-20140099863-A |
titleOfInvention | Process for preparing trialkyl compounds of metals of group iiia |
abstract | The present invention relates to a process for the preparation of a compound of the formula I R 3 M wherein M = a group IIIA metal of the Periodic Table of the Elements (PTE), preferably gallium or indium, and R = C 1 -C 5 -alkyl, preferably methyl or ethyl And a method for producing an alkyl metal compound. The process is based on the reaction of a metal trichloride (MeCl 3 ) with an alkyl aluminum sesquichloride (R 3 Al 2 Cl 3 ) in the presence of at least one alkyll metal halide as an auxiliary base. The trialkyl metal compound is separated from the reaction mixture through a separator, while the reaction mixture is heated to a temperature above 120 ° C and the partial alkylation product is recycled to the reaction mixture at the same time. In a further step, the reaction mixture is heated to a maximum of 350 < 0 > C and the remaining alkylated and partially alkylated products are separated. The product obtained in this way can optionally be recycled to the process. The method shows a high yield of trialkyl metal compound and also a high metal utilization; The product is used as a precursor for the MOCVD process. |
priorityDate | 2011-11-28-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 75.