http://rdf.ncbi.nlm.nih.gov/pubchem/patent/KR-20130096353-A

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filingDate 2012-02-22-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_dc3aeee81776569b029ca508c8457615
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publicationDate 2013-08-30-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber KR-20130096353-A
titleOfInvention Method for synthesizing dinitro derivative using optical shock and reaction device therefor
abstract Disclosed are a method for synthesizing a dinitro derivative using an optical shock and a reaction apparatus therefor. The reaction solution A is prepared by dissolving the metal chloride nitro compound monomer in the first solvent. Reaction solution B is prepared by dissolving the halogenated nitro compound monomer in a second solvent. The reaction solution A and the reaction solution B are taken in such a manner that the molar ratio of the monomer is in the range of 0.8: 1.0 to 1.0: 1.2, and the third solvent is added. The dinitro derivative is synthesized by applying a light shock while refluxing the mixture. Dinitro derivatives can be synthesized in high yields in a short time and are easy to industrialize.
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