http://rdf.ncbi.nlm.nih.gov/pubchem/patent/KR-20130078583-A

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filingDate 2011-12-30-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_2a36fa92a56627b8f08fe4bca8ca7b56
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publicationDate 2013-07-10-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber KR-20130078583-A
titleOfInvention Method of manufacturing poly(m-phenylene terephthal amide
abstract PURPOSE: A manufacturing method of a poly m-phenylene terephthal amide composition is provided to have an excellent heat resistance and a high intensity by polymerizing m-phenylenediamine and terephthaloyl chloride at low temperature. CONSTITUTION: A manufacturing method of a poly m-phenylene terephthal amide composition includes a dissolution step which dissolves m-phenylenediamine in N-methylpyrrolidone which includes CaCl2 which is a solvent; a polymerizing step which performs a polymerization by adding terephthaloyl chloride to N-methylpyrrolidone in which the m-phenylenediamine is dissolved; and a neutralization step which performs neutralization by adding CaO after the polymerization. The m-phenylenediamine is vacuum-sublimated in 0.1-1 torr and has 99% of purity. [Reference numerals] (AA) Dissolving step; (BB) Polymerizing step; (CC) Neutralizing step
priorityDate 2011-12-30-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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