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filingDate 2009-04-09-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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publicationDate 2011-01-13-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber KR-20110004403-A
titleOfInvention Method of manufacturing photocrosslinkable composition
abstract The present invention relates to (a) an organic-inorganic hybrid, in which all or almost all of the alkoxysilane groups are hydrolyzed and contain an average of at least four (epoxycycloalkyl) alkyl groups, preferably 4 to 10 (epoxycycloalkyl) alkyl groups, per molecule. In order to obtain a solution of the prepolymer, by heating the solution at a temperature of 50 to 70 ℃ for a period of 180 to 350 minutes, in an organic aqueous medium containing water in the initial water / monomer molar ratio of 3 to 15 and at least one aqueous solvent Causing hydrolysis and condensation reaction of [(epoxycycloalkyl) alkyl] trialkoxysilane in solution at a pH of 1.6 to 4.0, preferably 1.6 to 3.0; (b) cooling the resulting polyepoxide prepolymer composition to a temperature of 15-25 ° C .; (c) adding to the composition at least one cationic polymerization photoinitiator and at least one photosensitizer having a maximum absorbance at wavelengths of 300 to 420 nm and optionally a surfactant; (d) stirring the resulting composition at a temperature of 15-25 ° C. for a period of 10-120 minutes, preferably 20-40 minutes; (e) filtering the resulting composition through a filter comprising pores having an average size of 1 to 5 μm; And (f) storing the resulting liquid filtrate at a temperature of 0 ° C. or lower, preferably −20 ° C. to −10 ° C .. The invention also relates to the use of such photocrosslinkable compositions as negative photosensitive resins in photolithography processes.
priorityDate 2008-04-11-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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