http://rdf.ncbi.nlm.nih.gov/pubchem/patent/KR-20090124958-A

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filingDate 2009-05-27-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_ff188447984a6b355ee8b458d0c9947e
http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_382ae1298615c7a5a08d3bffc8730890
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publicationDate 2009-12-03-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber KR-20090124958-A
titleOfInvention Method of producing polyamide
abstract In a batch production method of a polyamide formed by directly polycondensing a diamine component containing a paraxylylenediamine and a dicarboxylic acid component using a batch reactor equipped with a splitting machine, a method for producing economically and qualityly advantageously to provide.n n n A diamine component and a dicarboxylic acid component containing 70 mol% or more of xylylenediamine containing 20 mol% or more of paraxylylenediamine in the absence of a real solvent using a batch reactor equipped with a partial condenser A method for producing a polyamide formed by direct polycondensation, the method for producing a polyamide comprising the following steps.n n n (1) A step of adding a dicarboxylic acid component to the reaction tank, followed by pressurizing the pressure in the reaction tank to a pressure of 0.1 MPaG or more.n n n (2) A step of continuously or intermittently adding the diamine component to the dicarboxylic acid component while maintaining the pressure in the reaction tank at a pressure of 0.1 MPaG or more and maintaining the uniform flow state of the entire reaction system.n n n (3) A step of reducing the pressure in the reaction tank to an atmospheric pressure or lower at a pressure drop rate of 0.1 to 1.0 MPa / hour after the addition of the diamine component is completed.
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priorityDate 2008-05-29-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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