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filingDate 2006-05-03-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_3361782b6d616a509803d20242affaec
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publicationDate 2008-01-18-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber KR-20080007390-A
titleOfInvention Method for separating methylglycinenitrile-N, N-diacetonitrile from aqueous crude mixture
abstract The present invention relates to a process for separating MGDN in a crystallizer from an aqueous emulsion containing MGDN having a content of methylglycinenitrile-N, N-diacetonitrile (MGDN) of 3-50% by weight. The process of the present invention comprises the steps of (a) cooling the aqueous emulsion to a temperature below the freezing point until the entire emulsified MGDN is substantially solidified, wherein the average cooling rate over time is 5 Not exceeding K / h, and (b) further cooling and / or concentrating the resulting aqueous suspension and allowing the cooling rate to be greater than the cooling rate of step (a). .
priorityDate 2005-05-06-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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