http://rdf.ncbi.nlm.nih.gov/pubchem/patent/KR-20080001653-A

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http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C209-48
filingDate 2007-06-28-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_6272fd43ef0b9c5f3df03b02e7af92b7
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publicationDate 2008-01-03-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber KR-20080001653-A
titleOfInvention How to prepare xylylenediamine
abstract The present invention relates to a process for the preparation of xylylenediamine by two stage hydrogenation of raw material phthalonitrile in a solvent. The main steps of the invention are the first hydrogenation step and the second hydrogenation step. In a first hydrogenation step, a raw phthalonitrile solution in a solvent comprising liquid ammonia is fed to the inlet of the first reaction zone, and hydrogenation is carried out in the first reaction zone in the presence of a heterogeneous catalyst, thereby producing the raw phthalonitrile. The nitrile group in it is hydrogenated with an aminomethyl group. A portion of the hydrogenation product solution from the first reaction zone is circulated to the inlet of the first reaction zone and the remainder is introduced into a second hydrogenation step where further hydrogenation proceeds.
isCitedBy http://rdf.ncbi.nlm.nih.gov/pubchem/patent/KR-20180077178-A
priorityDate 2006-06-29-04:00^^<http://www.w3.org/2001/XMLSchema#date>
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