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filingDate 1995-10-16-04:00^^<http://www.w3.org/2001/XMLSchema#date>
grantDate 2003-06-02-04:00^^<http://www.w3.org/2001/XMLSchema#date>
inventor http://rdf.ncbi.nlm.nih.gov/pubchem/patentinventor/MD5_b003febc9bbdc50000a3691778783ac2
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publicationDate 2003-06-02-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber KR-100374757-B1
titleOfInvention Polynitration of Aromatic Compounds
abstract The present invention relates to a polynitration method of an aromatic compound by continuous treatment with an emulsion as a reaction medium in an integrated apparatus under adiabatic conditions. 1.3 to 3.5 moles of HNO 3 per mole of aromatic compound are introduced into the reactor under conditions such that they form an emulsion with the aromatic compound in the form of a nitronium ion solution. Emulsions that tend to coalesce are maintained by repeated dispersion. The initial dispersion time of the liquid stream for preparing the emulsion is less than 1 second. In general, at least 20% of the total amount of HNO 3 used should be present during the initial dispersion. However, in the initial dispersion of the aromatic compound and the nitronium ion solution, it is preferable that the total amount of the nitronium ion solution used is present.
priorityDate 1994-10-17-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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