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filingDate 2012-04-03-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2015-02-23-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber JP-WO2012169274-A1
titleOfInvention Nickel composite hydroxide and production method thereof, positive electrode active material for non-aqueous electrolyte secondary battery, production method thereof, and non-aqueous electrolyte secondary battery
abstract Provided are a positive electrode active material having an appropriate particle size and high particle size uniformity, and a nickel composite hydroxide as a precursor thereof. When obtaining a nickel composite hydroxide by a crystallization reaction, a nucleation aqueous solution containing at least a nickel-containing metal compound and an ammonium ion supplier has a pH value of 12. on the basis of a liquid temperature of 25 ° C. After performing nucleation by controlling to be 0 to 14.0, the aqueous solution for particle growth containing the formed nuclei has a pH value of 10.5 to 12.0 based on a liquid temperature of 25 ° C., and The particles are grown by controlling the pH value to be lower than the pH value in the nucleation step. At this time, at least in the nucleation step, the oxygen concentration is 1% by volume or less in a non-oxidizing atmosphere in the range exceeding 40% of the whole particle growth step time from the start of the particle growth step. The power for the stirrer per unit volume is controlled to 0.5-4 kW / m 3 . [Selection] Figure 1
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priorityDate 2011-06-07-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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