http://rdf.ncbi.nlm.nih.gov/pubchem/patent/JP-WO2012132991-A1
Outgoing Links
Predicate | Object |
---|---|
classificationCPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D263-44 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07D263-22 http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C219-18 |
classificationIPCInventive | http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07D263-44 |
filingDate | 2012-03-19-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationDate | 2014-07-28-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
publicationNumber | JP-WO2012132991-A1 |
titleOfInvention | Glutamic acid benzyl ester N-carboxylic anhydride |
abstract | It is an object of the present invention to provide a crystalline polymorph having a high bulk density of the crystalline polymorphs of glutamic acid benzyl ester N-carboxylic anhydride and having excellent storage stability. To do. According to the present invention, glutamic acid benzyl ester N-carboxylic anhydride is dissolved in 0.5 L or more of solvent per mole of glutamic acid benzyl ester N-carboxylic anhydride heated to a temperature of 40 ° C. or more and less than boiling point, The bulk density is 0.45 g / cm 3 by adding 1.4 L or more poor solvent per mole of glutamic acid benzyl ester N-carboxylic anhydride at a temperature, precipitating crystals at a temperature of 40 ° C. or higher and lower than the boiling point, and cooling. The above crystalline polymorph of glutamic acid benzyl ester N-carboxylic anhydride could be obtained. |
priorityDate | 2011-03-25-04:00^^<http://www.w3.org/2001/XMLSchema#date> |
type | http://data.epo.org/linked-data/def/patent/Publication |
Incoming Links
Total number of triples: 39.