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http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C67-03
http://rdf.ncbi.nlm.nih.gov/pubchem/patentcpc/C07C67-54
classificationIPCInventive http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C67-03
http://rdf.ncbi.nlm.nih.gov/pubchem/patentipc/C07C69-54
filingDate 2004-02-03-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationDate 2006-05-25-04:00^^<http://www.w3.org/2001/XMLSchema#date>
publicationNumber JP-WO2004069783-A1
titleOfInvention Method for producing methacrylate ester
abstract Using a reactor equipped with a distillation column, the transesterification reaction between methyl methacrylate and alcohol or phenols was carried out while removing methanol produced as a by-product under reflux conditions as an azeotrope with methyl methacrylate. In the method for producing a methacrylic acid ester, when the temperature in the distillation column is converted to a temperature at normal pressure, the uppermost temperature is 63 to 68 ° C, the intermediate temperature is 68 to 90 ° C, and the lowermost temperature is After the temperature reaches 90 to 100 ° C., the azeotropic mixture of methanol and methyl methacrylate is started to be removed from the system, and when the conversion rate of alcohol or phenol is in the range of 0 to 95%, the distillation column By controlling the reflux ratio so as to maintain the internal temperature, the methacrylic acid ester is produced with high productivity.
priorityDate 2003-02-07-04:00^^<http://www.w3.org/2001/XMLSchema#date>
type http://data.epo.org/linked-data/def/patent/Publication

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